Related Links:
High Temperature Testing

All mechanical properties change as the temperature of the materials elevates. Micro Materials Ltd are the first to offer a hot stage which allows depth sensing nanoindentation tests to be performed at temperature of up to 750°C.
This opens up a vast range of new possibilities in surface and thin-film technology as it allows the measurement and optimisation of mechanical properties at service temperatures rather than relying on the extrapolation of results from room temperature.
Techniques possible at elevated temperatures
NanoTest MicroTest
Nanoindentation Microindentation
Nano-scratch and wear Micro-scratch and wear
Nano-impact and fatigue Micro-impact and fatigue
Excellent system stability at elevated temperatures
Due to the unique pendulum system employed by the NanoTest, MML are able to use a localised insulated heating system. This restricts the high temperatures to the indenter and sample area only. The technique means that the stages and electronics remain at room temperature, thus avoiding unwanted expansion/ contraction of the stages as the temperature changes, and retaining our industry leading low thermal drift.
Isothermal ContactTM
Micro Materials are the only manufacturer to offer tip heating as well as heating of the sample. This means that on indentation, there is no heat exchange between the tip and the sample, again avoiding possible sources of error due to sample or tip expansion/ contraction due to fluctuations in temperature.
Further Reading
High temperature application note (287kB PDF)
Measurement and modelling of the nanoindentation response of shape memory alloys. AJ Muir Wood, TW Clyne, Acta Materialica 2006(54) 5607-5615
High-temperature creep and hardness of eutectic 80Au/20Sn solder. YC Liu, JWR Teo, SK Tung, KH Lam, Journal of Alloys and Compounds 2007
Nanoindentation creep and glass transition
temperatures in polymers. BD
Beake
GA Bell, W Brostow, W Chonkaew, Polymer International 2007 (56)
773-778
Effect of mechanical properties measured at room and elevated temperature on the wear resistance of cutting tools and with TiAlN and AlCrN coatings. GS Fox-Rabinovich, BD Beake, JL Endrino, SC Veldhuis, R Parkinson, LS Shuster, MS Migranov, Surface and Coatings Technology, 2006 (200) 5738-5742.