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Application Note

Nano-Scale Wear Testing:

NanoTest Repetitive Scratch Test

NanoTest Repetitive Scratch Test


In the NanoTest, abrasive wear performance of a coating can be investigated by means of a multi-pass scratch test. This procedure consists of sequential constant load scratches over the same track, with a low load topography measurement performed between each scratch. In this way, changes in depth and friction can be monitored simultaneously.


Clearly, the success of such a procedure depends on the ability to precisely and automatically relocate the stylus at the same starting point prior to each step.

Case Study: Scratching Wear of Hydroxyapatite on Ti Alloy

Experimental

 

The following NanoTest results were obtained from a hydroxylapatite coating deposited on a titanium alloy. After an initial topography determination, 14 sequential friction measurements were carried out, with a topography measurement being performed between each one. For each scratch, a constant load of 75 mN was applied abruptly at the same point along the path of the stylus. A 120° conical diamond probe was used, with a tip radius of 25 µm.

Results

 

For the scratched area, the three figures show: (1) the actual topography evolution with continued scratching; (2) a progressive increase in plastic depth with sequential scratching; and (3) the occurrence of a maximum frictional force during the scratching sequence.

 

The first two figures show a significant change in average wear rate with an increasing number of scratches. Essentially, this increased significantly after the first few passes, with the maximum rate corresponding to the maximum frictional force. The results are indicative of different wear mechanisms, such as initial film cohesion failure followed by adhesion failure.

 

Fig.2

Displacement (nm)

vs. scratch number

 

 

 

 

 

 

Fig. 3

Frictional Force (mN)

vs. scratch number.