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Introduction
Transient elastic waves can be
generated in a region of a material which experiences abrupt changes in
stress or strain. This phenomenon is known as acoustic emission and is
generally detected by means of ultrasonic transducers coupled to the
material. Growth of microcracks, interfacial bond failure in fibre composite
materials, and delamination of a thin film are typical examples of events
which produce acoustic emission, although the acoustic radiation details
generally depend on the particular mechanism involved.
Acoustic emission frequencies are
usually in the range 150 - 300 kHz, that is, well above the frequency of
audible sound. This permits all ambient noise to be filtered out, to leave
only the frequencies of interest.
NanoTest/MicroTest Measurement System
In the NanoTest and MicroTest,
acoustic emission is detected by means of a piezoelectric transducer which
is mounted in such a way that its resonant frequency is in the range of the
signal of interest (> 200 kHz). The transducer element is mounted inside the
specimen holder. This is considered superior to the alternative approach of
mounting the transducer on the diamond holder since some acoustic emission
events can occur during diamond unloading, when the diamond may not be
effectively mechanically coupled to the specimen.
The main system components are shown
schematically. The bandpass amplifier eliminates ambient noise, mains
interference and very high frequency noise.
Because acoustic emission signals are generally very
fast, the signal is fed through a threshold detection and integration unit
which produces an analogue pulse proportional to the energy content of the
sensor output voltage. The voltage level at which a signal is accepted (that
is, the system sensitivity) is set prior to data acquisition.
Experimental
The example shows acoustic emission from a silicon
surface during a MicroTest scratch test. Since this was a low load
measurement, a relatively sharp 120o conical diamond was used. This had a
tip radius of approximately 20 µm. In this particular type of measurement,
the applied force is increased linearly (read from the right-hand axis), and
the acoustic emission is monitored continuously. A critical load for
scratching (or adhesion failure in the case of a thin film) is manifested
through a burst of acoustic emission.
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